IndiumV3, Main, Repository, bibRecord, 000824

Novel microwave assisted synthesis of ZnS nanomaterials

Identifieur interne : 000824 ( Main/Repository ); précédent : 000823; suivant : 000825

Novel microwave assisted synthesis of ZnS nanomaterials

Auteurs : RBID : Pascal:13-0090728

Descripteurs français

Pascal (Inist)
- Hyperfréquence, Synthèse nanomatériau, Semiconducteur II-VI, Indium, Diffraction RX, Spectre RX, Spectre photoélectron UV, Spectre UV visible, Spectre photoélectron RX, Luminescence, Propriété optique, Dimension particule, Défaut cristallin, Structure bande, Sulfure de zinc, Argent, Réseau cubique, Réseau hexagonal, Oxyde de zinc, Bande interdite, Niveau énergie, Propriété électronique, Activité catalytique, Photocatalyse, Transition phase, Etude comparative, Effet rayonnement, Oxyde de titane, ZnS, In, ZnO, TiO2, 6146, 8116, 7321, 6470N.
Wicri :
- concept : Argent.

English descriptors

KwdEn :
- Band structure, Catalyst activity, Comparative study, Crystal defects, Cubic lattices, Electronic properties, Energy gap, Energy levels, Hexagonal lattices, II-VI semiconductors, Indium, Luminescence, Microwave radiation, Nanomaterial synthesis, Optical properties, Particle size, Phase transitions, Photocatalysis, Radiation effects, Silver, Titanium oxide, Ultraviolet photoelectron spectra, Ultraviolet visible spectrum, X-ray photoelectron spectra, X-ray spectra, XRD, Zinc oxide, Zinc sulfide.

Abstract

A novel ambient pressure microwave assisted technique is developed in which silver and indium-modified ZnS is synthesized. The as-prepared ZnS is characterized by x-ray diffraction, UV-vis spectroscopy, x-ray photoelectron spectroscopy and luminescence spectroscopy. This procedure produced crystalline materials with particle sizes below 10 nm. The synthesis technique leads to defects in the crystal which induce mid-energy levels in the band gap and lead to indoor light photocatalytic activity. Increasing the amount of silver causes a phase transition from cubic blende to hexagonal phase ZnS. In a comparative study, when the ZnS cubic blende is heated in a conventional chamber furnace, it is completely converted to ZnO at 600 °C. Both cubic blende and hexagonal ZnS show excellent photocatalytic activity under irradiation from a 60 W light bulb. These ZnS samples also show significantly higher photocatalytic activity than the commercially available TiO₂ (Evonik-Degussa P-25).

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Pascal:13-0090728

Le document en format XML

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<author><name sortKey="Synnott, Damian W" uniqKey="Synnott D">Damian W. Synnott</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Centre for Research in Engineering Surface Technology (CREST), FOCAS Institute, Dublin Institute of Technology, Kevin Street</s1>
<s2>Dublin 8</s2>
<s3>IRL</s3>
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<country>Irlande (pays)</country>
<wicri:noRegion>Dublin 8</wicri:noRegion>
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<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>School of Chemical and Pharmaceutical Sciences, Dublin Institute of Technology, Kevin St.</s1>
<s2>Dublin 8</s2>
<s3>IRL</s3>
<sZ>1 aut.</sZ>
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<country>Irlande (pays)</country>
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<author><name sortKey="Seery, Michael K" uniqKey="Seery M">Michael K. Seery</name>
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<author><name sortKey="Hinder, Steven J" uniqKey="Hinder S">Steven J. Hinder</name>
<affiliation wicri:level="1"><inist:fA14 i1="03"><s1>School of Engineering, University of Surrey</s1>
<s2>Guildford, Surrey, GU2 7XH</s2>
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<country>Royaume-Uni</country>
<wicri:noRegion>Guildford, Surrey, GU2 7XH</wicri:noRegion>
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</author>
<author><name sortKey="Colreavy, John" uniqKey="Colreavy J">John Colreavy</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Centre for Research in Engineering Surface Technology (CREST), FOCAS Institute, Dublin Institute of Technology, Kevin Street</s1>
<s2>Dublin 8</s2>
<s3>IRL</s3>
<sZ>1 aut.</sZ>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
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<country>Irlande (pays)</country>
<wicri:noRegion>Dublin 8</wicri:noRegion>
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</author>
<author><name sortKey="Pillai, Suresh C" uniqKey="Pillai S">Suresh C. Pillai</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Centre for Research in Engineering Surface Technology (CREST), FOCAS Institute, Dublin Institute of Technology, Kevin Street</s1>
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<seriesStmt><idno type="ISSN">0957-4484</idno>
<title level="j" type="abbreviated">Nanotechnology : (Bristol, Print)</title>
<title level="j" type="main">Nanotechnology : (Bristol. Print)</title>
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</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Band structure</term>
<term>Catalyst activity</term>
<term>Comparative study</term>
<term>Crystal defects</term>
<term>Cubic lattices</term>
<term>Electronic properties</term>
<term>Energy gap</term>
<term>Energy levels</term>
<term>Hexagonal lattices</term>
<term>II-VI semiconductors</term>
<term>Indium</term>
<term>Luminescence</term>
<term>Microwave radiation</term>
<term>Nanomaterial synthesis</term>
<term>Optical properties</term>
<term>Particle size</term>
<term>Phase transitions</term>
<term>Photocatalysis</term>
<term>Radiation effects</term>
<term>Silver</term>
<term>Titanium oxide</term>
<term>Ultraviolet photoelectron spectra</term>
<term>Ultraviolet visible spectrum</term>
<term>X-ray photoelectron spectra</term>
<term>X-ray spectra</term>
<term>XRD</term>
<term>Zinc oxide</term>
<term>Zinc sulfide</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Hyperfréquence</term>
<term>Synthèse nanomatériau</term>
<term>Semiconducteur II-VI</term>
<term>Indium</term>
<term>Diffraction RX</term>
<term>Spectre RX</term>
<term>Spectre photoélectron UV</term>
<term>Spectre UV visible</term>
<term>Spectre photoélectron RX</term>
<term>Luminescence</term>
<term>Propriété optique</term>
<term>Dimension particule</term>
<term>Défaut cristallin</term>
<term>Structure bande</term>
<term>Sulfure de zinc</term>
<term>Argent</term>
<term>Réseau cubique</term>
<term>Réseau hexagonal</term>
<term>Oxyde de zinc</term>
<term>Bande interdite</term>
<term>Niveau énergie</term>
<term>Propriété électronique</term>
<term>Activité catalytique</term>
<term>Photocatalyse</term>
<term>Transition phase</term>
<term>Etude comparative</term>
<term>Effet rayonnement</term>
<term>Oxyde de titane</term>
<term>ZnS</term>
<term>In</term>
<term>ZnO</term>
<term>TiO2</term>
<term>6146</term>
<term>8116</term>
<term>7321</term>
<term>6470N</term>
</keywords>
<keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Argent</term>
</keywords>
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<front><div type="abstract" xml:lang="en">A novel ambient pressure microwave assisted technique is developed in which silver and indium-modified ZnS is synthesized. The as-prepared ZnS is characterized by x-ray diffraction, UV-vis spectroscopy, x-ray photoelectron spectroscopy and luminescence spectroscopy. This procedure produced crystalline materials with particle sizes below 10 nm. The synthesis technique leads to defects in the crystal which induce mid-energy levels in the band gap and lead to indoor light photocatalytic activity. Increasing the amount of silver causes a phase transition from cubic blende to hexagonal phase ZnS. In a comparative study, when the ZnS cubic blende is heated in a conventional chamber furnace, it is completely converted to ZnO at 600 °C. Both cubic blende and hexagonal ZnS show excellent photocatalytic activity under irradiation from a 60 W light bulb. These ZnS samples also show significantly higher photocatalytic activity than the commercially available TiO<sub>2</sub>
 (Evonik-Degussa P-25).</div>
</front>
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<fA08 i1="01" i2="1" l="ENG"><s1>Novel microwave assisted synthesis of ZnS nanomaterials</s1>
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<fA11 i1="02" i2="1"><s1>SEERY (Michael K.)</s1>
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<fA11 i1="03" i2="1"><s1>HINDER (Steven J.)</s1>
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<fA11 i1="05" i2="1"><s1>PILLAI (Suresh C.)</s1>
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<fA14 i1="01"><s1>Centre for Research in Engineering Surface Technology (CREST), FOCAS Institute, Dublin Institute of Technology, Kevin Street</s1>
<s2>Dublin 8</s2>
<s3>IRL</s3>
<sZ>1 aut.</sZ>
<sZ>4 aut.</sZ>
<sZ>5 aut.</sZ>
</fA14>
<fA14 i1="02"><s1>School of Chemical and Pharmaceutical Sciences, Dublin Institute of Technology, Kevin St.</s1>
<s2>Dublin 8</s2>
<s3>IRL</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
</fA14>
<fA14 i1="03"><s1>School of Engineering, University of Surrey</s1>
<s2>Guildford, Surrey, GU2 7XH</s2>
<s3>GBR</s3>
<sZ>3 aut.</sZ>
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</fA66>
<fC01 i1="01" l="ENG"><s0>A novel ambient pressure microwave assisted technique is developed in which silver and indium-modified ZnS is synthesized. The as-prepared ZnS is characterized by x-ray diffraction, UV-vis spectroscopy, x-ray photoelectron spectroscopy and luminescence spectroscopy. This procedure produced crystalline materials with particle sizes below 10 nm. The synthesis technique leads to defects in the crystal which induce mid-energy levels in the band gap and lead to indoor light photocatalytic activity. Increasing the amount of silver causes a phase transition from cubic blende to hexagonal phase ZnS. In a comparative study, when the ZnS cubic blende is heated in a conventional chamber furnace, it is completely converted to ZnO at 600 °C. Both cubic blende and hexagonal ZnS show excellent photocatalytic activity under irradiation from a 60 W light bulb. These ZnS samples also show significantly higher photocatalytic activity than the commercially available TiO<sub>2</sub>
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<fC02 i1="04" i2="3"><s0>001B60D70N</s0>
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<s5>01</s5>
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<fC03 i1="01" i2="3" l="ENG"><s0>Microwave radiation</s0>
<s5>01</s5>
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<s5>02</s5>
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<fC03 i1="02" i2="X" l="ENG"><s0>Nanomaterial synthesis</s0>
<s5>02</s5>
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<fC03 i1="02" i2="X" l="SPA"><s0>Síntesis nanomaterial</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="3" l="FRE"><s0>Semiconducteur II-VI</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG"><s0>II-VI semiconductors</s0>
<s5>03</s5>
</fC03>
<fC03 i1="04" i2="3" l="FRE"><s0>Indium</s0>
<s2>NC</s2>
<s5>04</s5>
</fC03>
<fC03 i1="04" i2="3" l="ENG"><s0>Indium</s0>
<s2>NC</s2>
<s5>04</s5>
</fC03>
<fC03 i1="05" i2="3" l="FRE"><s0>Diffraction RX</s0>
<s5>05</s5>
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<fC03 i1="05" i2="3" l="ENG"><s0>XRD</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="3" l="FRE"><s0>Spectre RX</s0>
<s5>06</s5>
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<fC03 i1="06" i2="3" l="ENG"><s0>X-ray spectra</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE"><s0>Spectre photoélectron UV</s0>
<s5>07</s5>
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<fC03 i1="07" i2="3" l="ENG"><s0>Ultraviolet photoelectron spectra</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="X" l="FRE"><s0>Spectre UV visible</s0>
<s5>08</s5>
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<fC03 i1="08" i2="X" l="ENG"><s0>Ultraviolet visible spectrum</s0>
<s5>08</s5>
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<fC03 i1="08" i2="X" l="SPA"><s0>Espectro UV visible</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>Spectre photoélectron RX</s0>
<s5>09</s5>
</fC03>
<fC03 i1="09" i2="3" l="ENG"><s0>X-ray photoelectron spectra</s0>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="3" l="FRE"><s0>Luminescence</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="3" l="ENG"><s0>Luminescence</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>Propriété optique</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>Optical properties</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE"><s0>Dimension particule</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG"><s0>Particle size</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE"><s0>Défaut cristallin</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="3" l="ENG"><s0>Crystal defects</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE"><s0>Structure bande</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG"><s0>Band structure</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE"><s0>Sulfure de zinc</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG"><s0>Zinc sulfide</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA"><s0>Zinc sulfuro</s0>
<s5>15</s5>
</fC03>
<fC03 i1="16" i2="3" l="FRE"><s0>Argent</s0>
<s2>NC</s2>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="3" l="ENG"><s0>Silver</s0>
<s2>NC</s2>
<s5>16</s5>
</fC03>
<fC03 i1="17" i2="3" l="FRE"><s0>Réseau cubique</s0>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="3" l="ENG"><s0>Cubic lattices</s0>
<s5>17</s5>
</fC03>
<fC03 i1="18" i2="3" l="FRE"><s0>Réseau hexagonal</s0>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="3" l="ENG"><s0>Hexagonal lattices</s0>
<s5>18</s5>
</fC03>
<fC03 i1="19" i2="X" l="FRE"><s0>Oxyde de zinc</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="X" l="ENG"><s0>Zinc oxide</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="X" l="SPA"><s0>Zinc óxido</s0>
<s5>19</s5>
</fC03>
<fC03 i1="20" i2="3" l="FRE"><s0>Bande interdite</s0>
<s5>29</s5>
</fC03>
<fC03 i1="20" i2="3" l="ENG"><s0>Energy gap</s0>
<s5>29</s5>
</fC03>
<fC03 i1="21" i2="3" l="FRE"><s0>Niveau énergie</s0>
<s5>30</s5>
</fC03>
<fC03 i1="21" i2="3" l="ENG"><s0>Energy levels</s0>
<s5>30</s5>
</fC03>
<fC03 i1="22" i2="X" l="FRE"><s0>Propriété électronique</s0>
<s5>31</s5>
</fC03>
<fC03 i1="22" i2="X" l="ENG"><s0>Electronic properties</s0>
<s5>31</s5>
</fC03>
<fC03 i1="22" i2="X" l="SPA"><s0>Propiedad electrónica</s0>
<s5>31</s5>
</fC03>
<fC03 i1="23" i2="X" l="FRE"><s0>Activité catalytique</s0>
<s5>32</s5>
</fC03>
<fC03 i1="23" i2="X" l="ENG"><s0>Catalyst activity</s0>
<s5>32</s5>
</fC03>
<fC03 i1="23" i2="X" l="SPA"><s0>Actividad catalítica</s0>
<s5>32</s5>
</fC03>
<fC03 i1="24" i2="X" l="FRE"><s0>Photocatalyse</s0>
<s5>33</s5>
</fC03>
<fC03 i1="24" i2="X" l="ENG"><s0>Photocatalysis</s0>
<s5>33</s5>
</fC03>
<fC03 i1="24" i2="X" l="SPA"><s0>Fotocatálisis</s0>
<s5>33</s5>
</fC03>
<fC03 i1="25" i2="X" l="FRE"><s0>Transition phase</s0>
<s5>34</s5>
</fC03>
<fC03 i1="25" i2="X" l="ENG"><s0>Phase transitions</s0>
<s5>34</s5>
</fC03>
<fC03 i1="25" i2="X" l="SPA"><s0>Transición fase</s0>
<s5>34</s5>
</fC03>
<fC03 i1="26" i2="X" l="FRE"><s0>Etude comparative</s0>
<s5>35</s5>
</fC03>
<fC03 i1="26" i2="X" l="ENG"><s0>Comparative study</s0>
<s5>35</s5>
</fC03>
<fC03 i1="26" i2="X" l="SPA"><s0>Estudio comparativo</s0>
<s5>35</s5>
</fC03>
<fC03 i1="27" i2="3" l="FRE"><s0>Effet rayonnement</s0>
<s5>36</s5>
</fC03>
<fC03 i1="27" i2="3" l="ENG"><s0>Radiation effects</s0>
<s5>36</s5>
</fC03>
<fC03 i1="28" i2="X" l="FRE"><s0>Oxyde de titane</s0>
<s5>37</s5>
</fC03>
<fC03 i1="28" i2="X" l="ENG"><s0>Titanium oxide</s0>
<s5>37</s5>
</fC03>
<fC03 i1="28" i2="X" l="SPA"><s0>Titanio óxido</s0>
<s5>37</s5>
</fC03>
<fC03 i1="29" i2="3" l="FRE"><s0>ZnS</s0>
<s4>INC</s4>
<s5>46</s5>
</fC03>
<fC03 i1="30" i2="3" l="FRE"><s0>In</s0>
<s4>INC</s4>
<s5>47</s5>
</fC03>
<fC03 i1="31" i2="3" l="FRE"><s0>ZnO</s0>
<s4>INC</s4>
<s5>48</s5>
</fC03>
<fC03 i1="32" i2="3" l="FRE"><s0>TiO2</s0>
<s4>INC</s4>
<s5>49</s5>
</fC03>
<fC03 i1="33" i2="3" l="FRE"><s0>6146</s0>
<s4>INC</s4>
<s5>65</s5>
</fC03>
<fC03 i1="34" i2="3" l="FRE"><s0>8116</s0>
<s4>INC</s4>
<s5>71</s5>
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   |texte=   Novel microwave assisted synthesis of ZnS nanomaterials
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Novel microwave assisted synthesis of ZnS nanomaterials

Novel microwave assisted synthesis of ZnS nanomaterials

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